TA Instruments

AR1756-0010f

15/03/2013 15:10:36

Sample name	ASW Blank coupon#20 + DI + beads 275rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	10 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:10:36

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0160	299.9	603.15	10000	20.0	0.2027	2.016	196.6	374.9	0.5244	825.8	295.7030	5.875E-3	369.63	36963	3.411E-3	0.0	0.0
2.0200	299.9	671.48	10000	20.0	0.1682	3.020	218.9	374.9	0.5838	685.3	547.0090	4.875E-3	683.76	68376	3.411E-3	0.0	0.1
3.0200	300.0	666.12	10000	20.0	0.1747	4.020	217.1	375.0	0.5790	711.7	796.9880	5.062E-3	996.24	99624	3.411E-3	0.1	0.1
4.0160	300.0	661.53	10000	20.0	0.1692	5.016	215.6	375.0	0.5750	689.4	1174.1600	4.902E-3	1467.7	1.4677E5	3.411E-3	0.1	0.1
5.0200	300.0	663.36	10000	20.0	0.1694	6.020	216.2	375.0	0.5766	690.3	1425.3800	4.908E-3	1781.7	1.7817E5	3.411E-3	0.1	0.1
6.0200	300.0	647.37	10000	20.0	0.1781	7.020	211.0	375.0	0.5627	725.8	1803.7800	5.161E-3	2254.7	2.2547E5	3.411E-3	0.1	0.1
7.0240	300.0	647.35	10000	20.0	0.1741	8.024	211.0	375.0	0.5627	709.3	2056.4399	5.044E-3	2570.6	2.5706E5	3.411E-3	0.1	0.1
8.0400	300.0	641.08	10000	20.0	0.1706	9.040	209.0	375.0	0.5572	695.2	2305.0000	4.944E-3	2881.3	2.8813E5	3.411E-3	0.1	0.2
9.0240	300.0	634.74	10000	20.0	0.1747	10.024	206.9	375.0	0.5517	711.7	2681.9299	5.062E-3	3352.4	3.3524E5	3.411E-3	0.2	0.2
10.016	300.0	630.90	10000	20.0	0.1729	11.016	205.6	375.0	0.5483	704.3	2933.2300	5.008E-3	3666.5	3.6665E5	3.411E-3	0.2	0.2
11.016	300.0	641.44	10000	20.0	0.1737	12.016	209.1	375.0	0.5576	707.6	3185.9199	5.032E-3	3982.4	3.9824E5	3.411E-3	0.2	0.2
12.060	300.0	643.06	10000	20.0	0.1739	13.060	209.6	375.0	0.5590	708.4	3561.6799	5.038E-3	4452.1	4.4521E5	3.411E-3	0.2	0.2
13.012	300.0	641.97	10000	20.0	0.1674	14.012	209.2	375.0	0.5580	682.0	3815.3301	4.850E-3	4769.2	4.7692E5	3.411E-3	0.2	0.2
14.020	300.0	644.78	10000	20.0	0.1816	15.020	210.2	375.0	0.5604	739.9	4189.9702	5.261E-3	5237.5	5.2375E5	3.411E-3	0.2	0.3
15.016	300.0	629.50	10000	20.0	0.1761	16.016	205.2	375.0	0.5471	717.5	4443.8398	5.102E-3	5554.8	5.5548E5	3.411E-3	0.3	0.3
16.016	300.0	630.87	10000	20.0	0.1737	17.016	205.6	375.0	0.5483	707.6	4694.1499	5.031E-3	5867.7	5.8677E5	3.411E-3	0.3	0.3
17.020	300.0	652.24	10000	20.0	0.1747	18.020	212.6	375.0	0.5669	711.7	5070.7402	5.062E-3	6338.4	6.3384E5	3.411E-3	0.3	0.3
18.016	300.0	630.73	10000	20.0	0.1692	19.016	205.6	375.0	0.5482	689.4	5322.9702	4.903E-3	6653.7	6.6537E5	3.411E-3	0.3	0.3
19.016	300.0	640.77	10000	20.0	0.1690	20.016	208.9	375.0	0.5570	688.6	5699.1401	4.897E-3	7123.9	7.1239E5	3.411E-3	0.3	0.3
20.016	300.0	637.77	10000	20.0	0.1690	21.016	207.9	375.0	0.5543	688.6	5949.3101	4.896E-3	7436.6	7.4366E5	3.411E-3	0.3	0.4
21.016	300.0	630.65	10000	20.0	0.1674	22.016	205.6	375.0	0.5481	682.0	6201.7798	4.849E-3	7752.2	7.7522E5	3.411E-3	0.4	0.4
22.016	300.0	632.62	10000	20.0	0.1818	23.016	206.2	375.0	0.5499	740.7	6577.6201	5.267E-3	8222.0	8.2220E5	3.411E-3	0.4	0.4
23.076	300.0	635.43	10000	20.0	0.1708	24.076	207.1	375.0	0.5523	696.0	6828.9502	4.949E-3	8536.2	8.5362E5	3.411E-3	0.4	0.4
24.016	300.0	643.76	10000	20.0	0.1702	25.016	209.8	375.0	0.5596	693.6	7080.2700	4.933E-3	8850.3	8.8503E5	3.411E-3	0.4	0.4
25.016	300.0	627.25	10000	20.0	0.1676	26.016	204.5	375.0	0.5451	682.8	7457.0298	4.855E-3	9321.3	9.3213E5	3.411E-3	0.4	0.4
26.020	300.0	639.86	10000	20.0	0.1688	27.020	208.6	375.0	0.5562	687.8	7715.1899	4.891E-3	9644.0	9.6440E5	3.411E-3	0.4	0.5
27.004	300.0	633.79	10000	20.0	0.1686	28.004	206.6	375.0	0.5509	686.9	8085.4702	4.885E-3	10107	1.0107E6	3.411E-3	0.5	0.5
28.020	300.0	630.84	10000	20.0	0.1704	29.020	205.6	375.1	0.5482	694.4	8336.8604	4.936E-3	10421	1.0421E6	3.411E-3	0.5	0.5
29.016	300.0	642.42	10000	20.0	0.1696	30.016	209.4	375.0	0.5584	691.1	8588.0703	4.914E-3	10735	1.0735E6	3.411E-3	0.5	0.5
30.020	300.0	622.98	10000	20.0	0.1690	31.020	203.1	375.0	0.5415	688.6	8966.4199	4.897E-3	11208	1.1208E6	3.411E-3	0.5	0.5
31.020	300.0	641.41	10000	20.0	0.1686	32.020	209.1	375.0	0.5575	686.9	9216.3896	4.885E-3	11520	1.1520E6	3.411E-3	0.5	0.5
32.024	300.0	648.09	10000	20.0	0.1686	33.024	211.2	375.0	0.5633	686.9	9593.6504	4.885E-3	11992	1.1992E6	3.411E-3	0.5	0.6
33.020	300.0	637.03	10000	20.0	0.1753	34.020	207.6	375.0	0.5537	714.2	9844.8604	5.079E-3	12306	1.2306E6	3.411E-3	0.6	0.6
34.024	300.0	645.20	10000	20.0	0.1702	35.024	210.3	375.0	0.5608	693.6	10101.200	4.931E-3	12627	1.2627E6	3.411E-3	0.6	0.6
35.016	300.0	631.97	10000	20.0	0.1645	36.016	206.0	375.0	0.5493	670.4	10477.500	4.767E-3	13097	1.3097E6	3.411E-3	0.6	0.6
36.020	300.0	639.79	10000	20.0	0.1672	37.020	208.5	375.0	0.5561	681.2	10724.700	4.844E-3	13406	1.3406E6	3.411E-3	0.6	0.6
37.016	300.0	643.13	10000	20.0	0.1672	38.016	209.6	375.0	0.5590	681.2	11105.700	4.843E-3	13882	1.3882E6	3.411E-3	0.6	0.6
38.016	300.0	635.00	10000	20.0	0.1706	39.016	207.0	375.0	0.5520	695.2	11352.800	4.944E-3	14191	1.4191E6	3.411E-3	0.6	0.7
39.028	300.0	652.08	10000	20.0	0.1723	40.028	212.5	375.0	0.5668	701.8	11604.000	4.991E-3	14505	1.4505E6	3.411E-3	0.7	0.7
40.016	300.0	632.50	10000	20.0	0.1761	41.016	206.2	375.0	0.5498	717.5	11981.700	5.103E-3	14977	1.4977E6	3.411E-3	0.7	0.7
41.016	300.0	636.08	10000	20.0	0.1694	42.016	207.3	375.0	0.5529	690.3	12234.900	4.908E-3	15294	1.5294E6	3.411E-3	0.7	0.7
42.028	300.0	636.07	10000	20.0	0.1700	43.028	207.3	375.0	0.5529	692.7	12483.800	4.926E-3	15605	1.5605E6	3.411E-3	0.7	0.7
43.004	300.0	625.17	10000	20.0	0.1792	44.004	203.8	375.0	0.5434	729.9	12862.200	5.190E-3	16078	1.6078E6	3.411E-3	0.7	0.7
44.016	300.0	616.75	10000	20.0	0.1755	45.016	201.0	375.0	0.5360	715.1	13112.100	5.084E-3	16390	1.6390E6	3.411E-3	0.7	0.8
45.020	300.0	634.77	10000	20.0	0.1714	46.020	206.9	375.0	0.5518	698.5	13489.000	4.968E-3	16861	1.6861E6	3.411E-3	0.8	0.8
46.016	300.0	640.60	10000	20.0	0.1668	47.016	208.8	375.0	0.5568	679.5	13740.500	4.832E-3	17176	1.7176E6	3.411E-3	0.8	0.8
47.020	300.0	627.83	10000	20.0	0.1743	48.020	204.6	375.0	0.5457	710.1	13994.200	5.049E-3	17493	1.7493E6	3.411E-3	0.8	0.8
48.004	300.0	643.16	10000	20.0	0.1702	49.004	209.6	375.0	0.5590	693.6	14368.700	4.932E-3	17961	1.7961E6	3.411E-3	0.8	0.8
49.008	300.0	650.03	10000	20.0	0.1688	50.008	211.9	375.0	0.5650	687.8	14620.000	4.891E-3	18275	1.8275E6	3.411E-3	0.8	0.8
50.016	300.0	645.13	10000	20.0	0.1700	51.016	210.3	375.0	0.5608	692.7	14998.900	4.927E-3	18749	1.8749E6	3.411E-3	0.8	0.9
51.016	300.0	639.40	10000	20.0	0.1643	52.016	208.4	375.0	0.5558	669.6	15249.500	4.762E-3	19062	1.9062E6	3.411E-3	0.9	0.9
52.004	300.0	634.59	10000	20.0	0.1643	53.004	206.8	375.0	0.5516	669.6	15499.800	4.762E-3	19375	1.9375E6	3.411E-3	0.9	0.9
53.008	300.0	640.96	10000	20.0	0.1712	54.008	208.9	375.0	0.5571	697.7	15876.700	4.961E-3	19846	1.9846E6	3.411E-3	0.9	0.9
54.004	300.0	630.62	10000	20.0	0.1749	55.004	205.5	375.0	0.5481	712.6	16128.000	5.067E-3	20160	2.0160E6	3.411E-3	0.9	0.9
55.004	300.0	619.55	10000	20.0	0.1775	56.004	201.9	375.0	0.5385	723.3	16379.400	5.143E-3	20474	2.0474E6	3.411E-3	0.9	0.9
56.012	300.0	631.33	10000	20.0	0.1708	57.012	205.8	375.0	0.5488	696.0	16759.301	4.950E-3	20949	2.0949E6	3.411E-3	0.9	1.0
57.004	300.0	640.60	10000	20.0	0.1700	58.004	208.8	375.0	0.5568	692.7	17009.199	4.927E-3	21262	2.1262E6	3.411E-3	1.0	1.0
58.020	300.0	644.91	10000	20.0	0.1702	59.020	210.2	375.0	0.5606	693.6	17387.699	4.933E-3	21735	2.1735E6	3.411E-3	1.0	1.0
59.004	300.0	638.66	10000	20.0	0.1706	60.004	208.2	375.0	0.5551	695.2	17636.000	4.943E-3	22045	2.2045E6	3.411E-3	1.0	1.0
60.016	300.0	639.91	10000	20.0	0.1652	61.016	208.6	375.0	0.5562	672.9	17889.699	4.785E-3	22362	2.2362E6	3.411E-3	1.0	1.0

